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Development and implication of methodology for aceclofenac in pure and pharmaceutical formulations by microwave assisted spectrophotometry

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dc.contributor.author Amina Mumtaz
dc.contributor.author Sattar, Asma Abdul
dc.contributor.author Rabia Nazir
dc.contributor.author Amjad Naseem
dc.date.accessioned 2023-01-19T09:42:12Z
dc.date.available 2023-01-19T09:42:12Z
dc.date.issued 2013-01-20
dc.identifier.citation Mumtaz, A., Sattar, A. A., Nazir, R., & Naseem, A. (2013). Development and implication of methodology for aceclofenac in pure and pharmaceutical formulations by microwave assisted spectrophotometry. Pakistan Journal of Pharmaceutical Sciences, 26(1). en_US
dc.identifier.issn 1011-601X
dc.identifier.uri http://142.54.178.187:9060/xmlui/handle/123456789/16116
dc.description.abstract A simple, fast and cost effective method for determination of Aceclofenac in pure and tablet formulations has been developed and validated. The method is based on formation of stable blue coloured complex (λmax = 740nm) of Aceclofenac with ammonium molybdate in presence of sulfuric acid under microwave irradiation for 5min. Peak shift in FT-IR spectra also indicated the formation of complex. Measurement of absorbance was carried out at λmax = 740nm. The reaction obeys Beer's law over the concentration range of 50-250µg/ml of Aceclofenac. The RSD (intra-day and inter-day precision) for the drug is not greater than 0.95% and recoveries were found to be in range of 99.01-99.99%. The proposed method can be used successfully for routine analysis of Aceclofenac in pure and tablet formulations. en_US
dc.language.iso en en_US
dc.publisher Karachi: Pakistan Botanical Society, University of Karachi en_US
dc.subject Aceclofenac en_US
dc.subject ammonium molybdate en_US
dc.subject microwave en_US
dc.subject FT-IR en_US
dc.subject spectrophotometry. en_US
dc.title Development and implication of methodology for aceclofenac in pure and pharmaceutical formulations by microwave assisted spectrophotometry en_US
dc.type Article en_US


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