dc.contributor.author |
WEI KE |
|
dc.contributor.author |
NA-BO SUN |
|
dc.contributor.author |
HONG-KE WU |
|
dc.date.accessioned |
2023-11-27T05:46:01Z |
|
dc.date.available |
2023-11-27T05:46:01Z |
|
dc.date.issued |
2013-08-09 |
|
dc.identifier.citation |
Ke, W., & Sun, N. B. (2013). Microwave assistant synthesis, crystal structure and biological activity of a 1, 2, 4-triazole compound. Journal of the Chemical Society of Pakistan, 35(4), 1241-1246. |
en_US |
dc.identifier.issn |
0253-5106 |
|
dc.identifier.uri |
http://142.54.178.187:9060/xmlui/handle/123456789/19971 |
|
dc.description.abstract |
The title compound (C₁₇H₁₄F₂N₄SO) were synthesized and recrystallized from CH₃CN. The compound was characterized by ¹H-NMR, FTIR, MS, HRMS and X-ray diffraction. The compound crystallized in the Monoclinic space group C2/c with a = 27.532(6), b = 8.9596(18), c = 14.609(3) Å, α = 90, β = 112.59(3), γ =90°, V = 3327.1(12) Å3, Z = 8 and R = 0.0327 for 2596 observed reflections with I > 2σ(I). X-ray analysis reveals that not only intermolecular N–H•••N interactions, but also C-H•••π stacking interactions exist in the adjacent molecules. The biological activities results showed that it exhibited significant herbicidal activity towards Brassica napus. |
en_US |
dc.description.sponsorship |
The chemical society of Pakistan is an approved society from the PSF. |
en_US |
dc.language.iso |
en |
en_US |
dc.publisher |
HEJ Research Institute of Chemistry, University of Karachi, Karachi. |
en_US |
dc.subject |
1,2,4-triazole |
en_US |
dc.subject |
synthesis |
en_US |
dc.subject |
herbicidal activity |
en_US |
dc.title |
Microwave Assistant Synthesis, Crystal Structure and Biological Activity of A 1,2,4-Triazole Compound |
en_US |
dc.type |
Article |
en_US |